X-ray powder diffractometer Rigaku SmartLab 3kW (RIGAKU3)


Guarantor:
Pavla Roupcová, Ph.D.

Instrument status:
Operational Operational, 9.5.2024 11:44, X-ray tube handling

Equipment placement:
CEITEC Nano - A1.16

Upcoming trainings:
6.6. 13:00 - 17:00: Rigaku3-základní - Bring your typical sample. A1.15 Go through: https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=429 https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=444
27.6. 13:00 - 17:00: Rigaku3-základní - Bring your typical sample. A1.15 Go through: https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=429 https://cfmoodle.ceitec.vutbr.cz/mod/lesson/view.php?id=444


X-Ray Powder Diffractometer equipped with Goebble mirror for HR spectra acquisition and JCPDS diffraction data database. In order to be able to observe temperature-dependent processes, a high temperature and low temperature chambers are planned as parts of the system.


Publications:

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Photogallery

Specification

Radiationfine focus Cu sealed tube; 40kV, 30mA
Goniometerθ/θ or θs, θd independent optical encoder controlled
radius 300 mm
Eulerian craddle (φ, Ω)
Incident opticsCBO, automatic variable divergence slit (BB, PB)
Ge 2-bounce and 4-bounce monochromators
Receiving opticsPSA, Ge 2-bounce analyzer, automatic receiving slit
Detectorsproportional and linear (D-tex)
HTK-16N chamberup to 800°C; vacuum, air, inert gases
TTK 450 chamberdown to –193°C; vacuum, dry gases
XRK 900 chamberup to 900°C, various gases



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